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Laboratory X-ray imaging in material sciences
Koudelka_ml., Petr ; Kytýř, Daniel ; Jiroušek, O.
In recent decades, X-ray imaging and computed (micro)tomography (XCT) in particular have become common tools for volumetric inspection, visualization, and analysis of internal structure in materials from various fields [1]. In this lecture, we will explore various applications of laboratory X-ray imaging chains utilizing the combination of tomographical imaging with mechanical, thermal, or chemical loading of the irradiated sample in a so-called time-resolved imaging allowing for unprecedented insight into different phenomena driving fundamental processes encountered in various fields of material science. We will show that failure processes in engineering or geological materials [2] can be thoroughly studied by synergy of information from radiographical imaging and other methods including acoustic emission detection and optical measurements via high-speed visible-spectrum and thermal-imaging cameras, where the radiography provides important spatial information regarding deformation processes evolving within the tested samples that could not be obtained otherwise. The state-of-the-art the laboratory based imaging chains for investigation of dynamic response of materials under loading will be also discussed including high speed X-ray radiography utilizing a powerful X-ray source during high velocity impact as an approach suitable for inspection of an impacted sample. As an alternative to both conventional high-power sources and accelerator facilities, capabilities of a flash X-ray system developed primarily for in-situ ballistics research providing very short bursts of an extremely powerful intermittent X-ray radiation with a typical duration of dozens of nanoseconds will be shown.
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3D PRINTED ARTIFICIAL MATERIALS FOR MICROWAVE STRUCTURES
Kaděra, Petr ; Soh, Ping Jack (oponent) ; Polívka, Milan (oponent) ; Láčík, Jaroslav (vedoucí práce)
The dissertation thesis deals with the research of 3D printed artificial electromagnetic structures exploitable for antenna and microwave component design. Artificial structures containing dielectric and metallic inclusions of various geometries are investigated, and their precise description, including the anisotropy effect, can improve the actual design speed and accuracy. First, the models based on the analytical parallel plate capacitor method are compared with an effective medium theory, numerical, and experimental results, which are provided for various parameters of materials available in 3D printing technology. The proposed models derived by the parallel plate capacitor method can generally be exploited for faster and highly accurate determination of the effective complex permittivity, which enhances its potential to be used with optimization techniques. Second, the hybrid multimodal transfer matrix method is exploited as a general and effective way for calculations of the effective permittivity and effective permeability of artificial structures containing both dielectric and metallic inclusions through the volumetric space of the structures studied. The artificial structures containing metallic inclusions generally allow to achieve a wide tuning range of the effective constitutive parameters. Finally, suitable structures with spatial permittivity distribution are developed for wide-angle millimeter-wave gradient-index Luneburg lenses employable as antennas or retroreflectors for wide angular coverage and stable radar cross section enhancements of passive, chipless frequency-coded radiofrequency identification tag landmarks which have a large potential for indoor self-localization.
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Zpráva o výsledcích mikroskopické analýzy malt použitých pro opravu vnější omítky objektu Petschkova vila, V sadech 2, Praha 6
Slížková, Zuzana ; Koudelková, Veronika ; Frankeová, Dita ; Šterner, Adam
Cílem práce bylo zjištění složení opravné malty použité na fasádě Petschkovy vily, V sadech 2, Praha 6 za účelem průzkumu fasády vily před restaurováním. Bylo provedeno SEM-EDX vyšetření nábrusu malty, výsledkem je charakterizace kameniva a pojiva malty. Pomocí analýz bylo určeno, že se jedná o cementovou maltu překrytou vápenocementovým štukem.
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Chemický a mikroskopický rozbor vnější omítky, Petschkova vila, V sadech 2, Praha 6
Slížková, Zuzana ; Viani, Alberto ; Koudelková, Veronika ; Frankeová, Dita ; Hauková, Petra
Cílem práce bylo provedení analýzy malty z Petschkovy vily, byly navrženy analýzy XRD a SEM-EDX, jejichž výsledkem je charakterizace kameniva a pojiva malt. Pomocí analýz bylo určeno, že se jedná o sádrovou omítku s nátěrem.
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